Third phase formation revisited: the U(VI), HNO 3 - TBP, n-dodecane systemĬhiarizia, R. The prepared compounds are grouped in the aqueous and organic phases As a result of TBP radiolysis except dibutyl phosphate and monobutylphosphate other compounds are prepared, which contain phosphorus in a molecule, besides, their quantity depends on the nitric acid concentration and the diluent type (n-dodecan, carbon tetrachloride, mesitylen), together with which TBP was irradiated. To separate the TBP decomposition products the thin layer chromatography method was used, and for the quantitative determination TBP, labelled with 32 P was used. Effects of the HNO 3 concentration and the diluent type upon the degree of the TBP decomposition in the system under investigation were determined as well. Phosphorus-containing compounds, prepared by radiolysis of the TBP-diluent-HNO 3 system, are determined quantitatively. International Nuclear Information System (INIS) Investigation into radiolysis of tbp labelled with 32P in the 30% tbp-diluent-HNO 3 systems
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